An easy electrochemical synthesis of 2-amino-4-aryl-3-cyano-5-ethoxycarbonyl-6-methyl-4H-pyrans has been set up, by galvanostatic electrolysis of a mixture of arylidenemalononitrile and ethyl acetoacetate in the absence of supporting electrolyte. Very high yields are obtained by a particularly simple procedure.
Sotgiu, G. (2008). Easy Electrochemical Synthesis of 2-amino-4-aryl-3-cyano-5-ethoxycar-bonyl-6-methyl-4H-pyrans in the Absence of Supporting Electrolyte. LETTERS IN ORGANIC CHEMISTRY, 5(7), 555-558 [10.2174/157017808785982202].
Easy Electrochemical Synthesis of 2-amino-4-aryl-3-cyano-5-ethoxycar-bonyl-6-methyl-4H-pyrans in the Absence of Supporting Electrolyte
SOTGIU, Giovanni
2008-01-01
Abstract
An easy electrochemical synthesis of 2-amino-4-aryl-3-cyano-5-ethoxycarbonyl-6-methyl-4H-pyrans has been set up, by galvanostatic electrolysis of a mixture of arylidenemalononitrile and ethyl acetoacetate in the absence of supporting electrolyte. Very high yields are obtained by a particularly simple procedure.File in questo prodotto:
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